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Título : | Complete assignment of the 1H and 13C NMR spectra of the tetraisoprenylated benzophenone 15-epiclusianone. |
Autor : | Santos, Marcelo Henrique dos Nagem, Tanus Jorge Braz Filho, Raimundo Lula, Ivana Silva Speziali, Nivaldo Lucio |
Fecha de publicación : | 2001 |
Citación : | SANTOS, M. H. dos et al. Complete assignment of the 1H and 13C NMR spectra of the tetraisoprenylated benzophenone 15-epiclusianone. Magnetic Resonance in Chemistry, Chichester, v. 39, n.3, p. 155-159, 2001. Disponível em: <http://onlinelibrary.wiley.com/doi/10.1002/mrc.795/full>. Acesso em: 20 mai. 2017. |
Resumen : | An NMR study of 15-epiclusianone, 1-benzoyl-6-hydroxy-14,14-dimethyl-3,5,15-tri(3-methyl-2-butenyl)- bicyclo[3.3.1]non-1-ene-4,6-dione (1), a novel tetraisoprenylated benzophenone isolated from pericarp of fruits of Rheedia gardneriana, is described. In addition to conventional 1D NMR techniques, 2D shiftcorrelated NMR experiments [1H 1H-COSY, 1H 13C-HMQC-1J(C,H), 1H 13C-HMBC-nJ(C,H) (n = 2 and 3) and 1H 1H-NOESY] were used for 1H and 13C chemical shift assignments of this natural product. The 1D 13C NMR spectrum of 1 in the solid state was also obtained. |
URI : | http://www.repositorio.ufop.br/handle/123456789/7948 |
metadata.dc.identifier.uri2: | http://onlinelibrary.wiley.com/doi/10.1002/mrc.795/full |
metadata.dc.identifier.doi: | https://doi.org/10.1002/mrc.795 |
ISSN : | 1097-458X |
Aparece en las colecciones: | DEQUI - Artigos publicados em periódicos |
Ficheros en este ítem:
Fichero | Descripción | Tamaño | Formato | |
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ARTIGO_CompleteAssignmentH.pdf Restricted Access | 170,79 kB | Adobe PDF | Visualizar/Abrir |
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