Complete assignment of the 1H and 13C NMR spectra of the tetraisoprenylated benzophenone 15-epiclusianone.

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dc.contributor.authorSantos, Marcelo Henrique dos
dc.contributor.authorNagem, Tanus Jorge
dc.contributor.authorBraz Filho, Raimundo
dc.contributor.authorLula, Ivana Silva
dc.contributor.authorSpeziali, Nivaldo Lucio
dc.date.accessioned2017-06-13T13:33:33Z
dc.date.available2017-06-13T13:33:33Z
dc.date.issued2001
dc.description.abstractAn NMR study of 15-epiclusianone, 1-benzoyl-6-hydroxy-14,14-dimethyl-3,5,15-tri(3-methyl-2-butenyl)- bicyclo[3.3.1]non-1-ene-4,6-dione (1), a novel tetraisoprenylated benzophenone isolated from pericarp of fruits of Rheedia gardneriana, is described. In addition to conventional 1D NMR techniques, 2D shiftcorrelated NMR experiments [1H 1H-COSY, 1H 13C-HMQC-1J(C,H), 1H 13C-HMBC-nJ(C,H) (n = 2 and 3) and 1H 1H-NOESY] were used for 1H and 13C chemical shift assignments of this natural product. The 1D 13C NMR spectrum of 1 in the solid state was also obtained.pt_BR
dc.identifier.citationSANTOS, M. H. dos et al. Complete assignment of the 1H and 13C NMR spectra of the tetraisoprenylated benzophenone 15-epiclusianone. Magnetic Resonance in Chemistry, Chichester, v. 39, n.3, p. 155-159, 2001. Disponível em: <http://onlinelibrary.wiley.com/doi/10.1002/mrc.795/full>. Acesso em: 20 mai. 2017.pt_BR
dc.identifier.doihttps://doi.org/10.1002/mrc.795
dc.identifier.issn1097-458X
dc.identifier.urihttp://www.repositorio.ufop.br/handle/123456789/7948
dc.identifier.uri2http://onlinelibrary.wiley.com/doi/10.1002/mrc.795/fullpt_BR
dc.language.isoen_USpt_BR
dc.rightsrestritopt_BR
dc.titleComplete assignment of the 1H and 13C NMR spectra of the tetraisoprenylated benzophenone 15-epiclusianone.pt_BR
dc.typeArtigo publicado em periodicopt_BR
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