Please use this identifier to cite or link to this item: http://www.repositorio.ufop.br/handle/123456789/5997
Title: Evaluation of short cycles of ultrasound application in nanoemulsions to obtain nanocapsules.
Authors: Carneiro, Simone Pinto
Cruz, Ricardo Machado
Santos, Orlando David Henrique dos
Keywords: Ultrasound polymerization
In situ polymerization
Nanocapsules
Issue Date: 2015
Citation: CARNEIRO, S. P.; CRUZ, R.M.; SANTOS, O. D. H. dos. Evaluation of short cycles of ultrasound application in nanoemulsions to obtain nanocapsules. Ultrasonics Sonochemistry, v. 27, p. 536-542, 2015. Disponível em: <http://www.sciencedirect.com/science/article/pii/S1350417715000826>. Acesso em: 15 out. 2015.
Abstract: Ultrasound is widely used in several chemical reactions and other process, including production of nanocapsules by in situ polymerization. In this work, the main objective was to evaluate the impacts and viability of successive ultrasound application in nanoemulsions to obtain nanocapsules. Initiator potassium persulfate (KPS) concentration, number of ultrasound cycles and reaction time influences on polymerization efficiency and droplet size were evaluated. This work revealed the successful in situ production of nanocapsules using successive shorts cycles of ultrasound. Number of cycles was the only parameter that not exerted significant influence in polymerization yield. Particle size decay was observed in all nanoemulsions after the first ultrasound application, the same was not observed in further cycles. Gravimetric assessment showed remarkable increase of monomer conversion, indicating that once started polymerization continued at least until 28 days after ultrasound application. Concluding, ultrasound short cycles can be used with no harm to formulation, if carefully performed and, furthermore is a potential cost-effective route for polymerization reactions
URI: http://www.repositorio.ufop.br/handle/123456789/5997
metadata.dc.identifier.doi: https://doi.org/10.1016/j.ultsonch.2015.04.002
ISSN: 1350-4177
metadata.dc.rights.license: O periódico Ultrasonics Sonochemistry concede permissão para depósito deste artigo no Repositório Institucional da UFOP. Número da licença: 3732420731744.
Appears in Collections:DEFAR - Artigos publicados em periódicos

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